DELONG INSTRUMENTS a.s.

Vacuum Furnaces

DI VP-1000 Laboratory Vacuum Furnaces

The furnace is intended for vacuum annealing and soldering.
Being made of austenitic stainless steel, the furnace features a double-jacket design; the inter-jacket space is flown through by cooling water. The furnace top cover accommodates a sight glass and two water-cooled vacuum-tight power-cable bushings. The furnace bottom cover is provided with two vacuum-tight bushings for thermocouple lead-in wires and a junction piece for the pumping unit valve. The top and the bottom covers are water-cooled, too.

The top cover and the jacket make up a bell in which a heating cage is mounted. The bell is sealed against the bottom cover by an O-ring. It can be lifted by means of a manually operated lifting gear.

The heating cage consists of an upper and a lower molybdenum annular ring systems and molybdenum heating rods, which are insulated by alumina rings. The space between the heating cage and the vacuum chamber water-cooled jackets is filled with five radiation-shielding layers, which are made of molybdenum, too.

A programmable controller, allowing easy programming of heating cycles, controls the low-voltage current heating system operation. Two independent thermocouple thermometers are used to measure the temperature.

A pumping set, consisting of a turbo-molecular pump and a membrane pump, provides vacuum in the chamber. The furnace operating chamber is insulated from the pumps by means of a slide valve; an anti-vacuum valve serves to fill the chamber with air or inert gas. Pirani and Penning gauges are used to measure the pressure.

The furnace cooling is provided by a steady flow-through of tap water, whose flow rate is measured by a flow meter.

Reliability, simple design and low space and power requirements are the most decisive advantages of this furnace.

Lifted Furnace Bell

Programmable Controller

 

Technical Specification

Heating
heating cage
Ø2 mm molybdenum rods
power supply
48 V / 100 A
Temperature measurement
temperature sensor
two thermocouples (K-type)
max. permissible temperature
1,100 °C
temperature measurement accuracy
±1 °C
temperature control thermocouple selection
both manual and automatic
Vacuum
operating pressure
ATM up to 3×10–6 mbar
vacuum pumps
– membrane
MVP 055-3
– turbo-molecular
EXT 255H
vacuometer
Pfeiffer Vacuum DualGauge TPG 262
vacuum gauges
Pfeiffer Compact Pirani Gauge TPR 265
Pfeiffer Compact Pirani Gauge TPR 251
Cooling
circulation, closed circuit recommended
cooling medium
water, reconditioned water recommended
recommended pressure
3 to 5 atm
consumption
~3 L min–1
cooling medium flow watching
automatic
cooling system temperature measurement
up to 125 °C
max. permissible operating temperature of the coolant
60 °C
Operation
maximum size of an object the furnace can accept
Ø130×170 mm
heat treatment temperature profile setting
programmable
number of programs
10 + the current one
number of temperature profile phases
up to 6
phase temperature setting range
actual temperature, 300 to 1050 °C
phase timing setting range
temperature hold time
10 to 1000 min
rise or fall rate
step 50 to 1,800 °C/h
supply voltage
3×230 V / 400 V ± 10 %, N+PE / 50 Hz
power demand
5 kVA
dimensions (h×w×d)
1550×600×1580 mm
weight
210 kg